<?xml version="1.0" encoding="UTF-8"?><toc><section id="sec_foreword"><title>Foreword</title></section><section id="body"><title>Hauptteil</title><section id="sec_1"><label>1</label><title>Scope</title></section><section id="sec_2"><label>2</label><title>Normative references</title></section><section id="sec_3"><label>3</label><title>Terms and definitions</title></section><section id="sec_4"><label>4</label><title>General considerations for sampling and sample preparation</title><section id="sec_4.1"><label>4.1</label><title>Basic requirements</title></section><section id="sec_4.2"><label>4.2</label><title>Establishing a sampling scheme</title></section><section id="sec_4.3"><label>4.3</label><title>System verification</title></section></section><section id="sec_5"><label>5</label><title>Fundamentals of sampling and sample preparation</title><section id="sec_5.1"><label>5.1</label><title>Minimization of bias</title><section id="sec_5.1.1"><label>5.1.1</label><title>General</title></section><section id="sec_5.1.2"><label>5.1.2</label><title>Minimization of particle size degradation</title></section><section id="sec_5.1.3"><label>5.1.3</label><title>Extraction of increments</title></section><section id="sec_5.1.4"><label>5.1.4</label><title>Increment mass</title><section id="sec_5.1.4.1"><label>5.1.4.1</label><title>General</title></section><section id="sec_5.1.4.2"><label>5.1.4.2</label><title>Increment mass for falling stream sampling</title></section><section id="sec_5.1.4.3"><label>5.1.4.3</label><title>Increment mass for stopped-belt sampling</title></section><section id="sec_5.1.4.4"><label>5.1.4.4</label><title>Increment mass for manual sampling using spear or auger</title></section></section></section><section id="sec_5.2"><label>5.2</label><title>Overall precision</title></section><section id="sec_5.3"><label>5.3</label><title>Quality variation</title></section><section id="sec_5.4"><label>5.4</label><title>Sampling precision and number of primary increments</title><section id="sec_5.4.1"><label>5.4.1</label><title>Mass-basis sampling</title></section><section id="sec_5.4.2"><label>5.4.2</label><title>Time-basis sampling</title></section></section><section id="sec_5.5"><label>5.5</label><title>Precision of sample preparation and overall precision</title><section id="sec_5.5.1"><label>5.5.1</label><title>General</title></section><section id="sec_5.5.2"><label>5.5.2</label><title>Preparation and measurement of gross sample</title></section><section id="sec_5.5.3"><label>5.5.3</label><title>Preparation and measurement of partial samples</title></section><section id="sec_5.5.4"><label>5.5.4</label><title>Preparation and measurement of each increment</title></section></section></section><section id="sec_6"><label>6</label><title>Methods of sampling</title><section id="sec_6.1"><label>6.1</label><title>Mass-basis sampling</title><section id="sec_6.1.1"><label>6.1.1</label><title>Mass of increment</title></section><section id="sec_6.1.2"><label>6.1.2</label><title>Quality variation</title></section><section id="sec_6.1.3"><label>6.1.3</label><title>Number of primary increments</title></section><section id="sec_6.1.4"><label>6.1.4</label><title>Sampling interval</title></section><section id="sec_6.1.5"><label>6.1.5</label><title>Methods of taking increments</title></section></section><section id="sec_6.2"><label>6.2</label><title>Time-basis sampling</title><section id="sec_6.2.1"><label>6.2.1</label><title>Mass of increment</title></section><section id="sec_6.2.2"><label>6.2.2</label><title>Quality variation</title></section><section id="sec_6.2.3"><label>6.2.3</label><title>Number of increments</title></section><section id="sec_6.2.4"><label>6.2.4</label><title>Sampling interval</title></section><section id="sec_6.2.5"><label>6.2.5</label><title>Methods of taking increments</title></section></section><section id="sec_6.3"><label>6.3</label><title>Stratified random sampling within fixed mass or time intervals</title><section id="sec_6.3.1"><label>6.3.1</label><title>General</title></section><section id="sec_6.3.2"><label>6.3.2</label><title>Fixed mass intervals</title></section><section id="sec_6.3.3"><label>6.3.3</label><title>Fixed time intervals</title></section></section></section><section id="sec_7"><label>7</label><title>Sampling from moving streams</title><section id="sec_7.1"><label>7.1</label><title>General</title></section><section id="sec_7.2"><label>7.2</label><title>Safety of operations</title></section><section id="sec_7.3"><label>7.3</label><title>Robustness of sampling installation</title></section><section id="sec_7.4"><label>7.4</label><title>Versatility of sampling system</title></section><section id="sec_7.5"><label>7.5</label><title>Primary samplers</title><section id="sec_7.5.1"><label>7.5.1</label><title>Location</title></section><section id="sec_7.5.2"><label>7.5.2</label><title>Types of primary sampler</title></section><section id="sec_7.5.3"><label>7.5.3</label><title>General design criteria for primary cutters</title></section><section id="sec_7.5.4"><label>7.5.4</label><title>Cutter aperture of primary sampler</title></section><section id="sec_7.5.5"><label>7.5.5</label><title>Cutter speed of primary sampler</title></section></section><section id="sec_7.6"><label>7.6</label><title>Secondary and subsequent samplers</title></section><section id="sec_7.7"><label>7.7</label><title>Online sample preparation</title><section id="sec_7.7.1"><label>7.7.1</label><title>Arrangement for sample preparation</title></section><section id="sec_7.7.2"><label>7.7.2</label><title>Crushers</title></section><section id="sec_7.7.3"><label>7.7.3</label><title>Dividers</title></section><section id="sec_7.7.4"><label>7.7.4</label><title>Dryers</title></section></section><section id="sec_7.8"><label>7.8</label><title>Checking precision and bias</title></section><section id="sec_7.9"><label>7.9</label><title>Cleaning and maintenance</title></section><section id="sec_7.10"><label>7.10</label><title>Example of a flowsheet</title></section></section><section id="sec_8"><label>8</label><title>Sampling from stationary situations</title><section id="sec_8.1"><label>8.1</label><title>General</title></section><section id="sec_8.2"><label>8.2</label><title>Sampling from trucks and wagons</title><section id="sec_8.2.1"><label>8.2.1</label><title>General </title></section><section id="sec_8.2.2"><label>8.2.2</label><title>Sampling devices</title></section><section id="sec_8.2.3"><label>8.2.3</label><title>Number of primary increments</title></section><section id="sec_8.2.4"><label>8.2.4</label><title>Method of sampling</title></section></section><section id="sec_8.3"><label>8.3</label><title>Sampling from ships, stockpiles and bunkers</title></section></section><section id="sec_9"><label>9</label><title>Stopped-belt reference sampling</title></section><section id="sec_10"><label>10</label><title>Sample preparation</title><section id="sec_10.1"><label>10.1</label><title>Fundamentals</title><section id="sec_10.1.1"><label>10.1.1</label><title>General</title></section><section id="sec_10.1.2"><label>10.1.2</label><title>Drying</title></section><section id="sec_10.1.3"><label>10.1.3</label><title>Crushing and grinding</title></section><section id="sec_10.1.4"><label>10.1.4</label><title>Mixing</title></section><section id="sec_10.1.5"><label>10.1.5</label><title>Division</title><section id="sec_10.1.5.1"><label>10.1.5.1</label><title>General</title></section><section id="sec_10.1.5.2"><label>10.1.5.2</label><title>Method of division</title></section><section id="sec_10.1.5.3"><label>10.1.5.3</label><title>Types of division</title></section><section id="sec_10.1.5.4"><label>10.1.5.4</label><title>Types of divider</title></section></section><section id="sec_10.1.6"><label>10.1.6</label><title>Mass of divided sample</title><section id="sec_10.1.6.1"><label>10.1.6.1</label><title>Division of chemical analysis and moisture samples</title><section id="sec_10.1.6.1.1"><label>10.1.6.1.1</label><title>Division of gross sample</title></section><section id="sec_10.1.6.1.2"><label>10.1.6.1.2</label><title>Division of individual increments or partial samples</title></section></section><section id="sec_10.1.6.2"><label>10.1.6.2</label><title>Division of size samples</title><section id="sec_10.1.6.2.1"><label>10.1.6.2.1</label><title>General</title></section><section id="sec_10.1.6.2.2"><label>10.1.6.2.2</label><title>Division of gross sample</title></section><section id="sec_10.1.6.2.3"><label>10.1.6.2.3</label><title>Division of increment or partial sample</title></section></section><section id="sec_10.1.6.3"><label>10.1.6.3</label><title>Division of samples for physical testing</title></section></section><section id="sec_10.1.7"><label>10.1.7</label><title>Split use and multiple use of sample</title></section></section><section id="sec_10.2"><label>10.2</label><title>Method of constituting partial samples or a gross sample</title><section id="sec_10.2.1"><label>10.2.1</label><title>General</title></section><section id="sec_10.2.2"><label>10.2.2</label><title>Method of constitution for mass-basis sampling</title><section id="sec_10.2.2.1"><label>10.2.2.1</label><title>Constitution of partial samples or a gross sample from increments</title></section><section id="sec_10.2.2.2"><label>10.2.2.2</label><title>Constitution of a gross sample from partial samples</title></section></section><section id="sec_10.2.3"><label>10.2.3</label><title>Method of constitution for time-basis sampling</title><section id="sec_10.2.3.1"><label>10.2.3.1</label><title>Constitution of partial samples or a gross sample from increments</title></section><section id="sec_10.2.3.2"><label>10.2.3.2</label><title>Constitution of a gross sample from partial samples</title></section></section><section id="sec_10.2.4"><label>10.2.4</label><title>Special procedure for moisture content</title></section></section><section id="sec_10.3"><label>10.3</label><title>Mechanical methods of division</title><section id="sec_10.3.1"><label>10.3.1</label><title>Mechanical increment division</title><section id="sec_10.3.1.1"><label>10.3.1.1</label><title>General</title></section><section id="sec_10.3.1.2"><label>10.3.1.2</label><title>Mass of increment (cut)</title></section><section id="sec_10.3.1.3"><label>10.3.1.3</label><title>Number of increments (cuts)</title></section><section id="sec_10.3.1.4"><label>10.3.1.4</label><title>Interval between cuts</title></section><section id="sec_10.3.1.5"><label>10.3.1.5</label><title>Avoiding bias</title></section><section id="sec_10.3.1.6"><label>10.3.1.6</label><title>Mass of divided sample</title></section></section><section id="sec_10.3.2"><label>10.3.2</label><title>Other mechanical division methods</title><section id="sec_10.3.2.1"><label>10.3.2.1</label><title>General</title></section><section id="sec_10.3.2.2"><label>10.3.2.2</label><title>Mass of divided sample</title></section></section></section><section id="sec_10.4"><label>10.4</label><title>Manual methods of division</title><section id="sec_10.4.1"><label>10.4.1</label><title>General</title></section><section id="sec_10.4.2"><label>10.4.2</label><title>Manual increment-division method</title><section id="sec_10.4.2.1"><label>10.4.2.1</label><title>General</title></section><section id="sec_10.4.2.2"><label>10.4.2.2</label><title>Mass of increment</title></section><section id="sec_10.4.2.3"><label>10.4.2.3</label><title>Number of increments</title></section><section id="sec_10.4.2.4"><label>10.4.2.4</label><title>Mass of divided sample</title></section><section id="sec_10.4.2.5"><label>10.4.2.5</label><title>Procedure</title></section></section><section id="sec_10.4.3"><label>10.4.3</label><title>Manual strip-division method</title><section id="sec_10.4.3.1"><label>10.4.3.1</label><title>General</title></section><section id="sec_10.4.3.2"><label>10.4.3.2</label><title>Mass of increment</title></section><section id="sec_10.4.3.3"><label>10.4.3.3</label><title>Number of increments</title></section><section id="sec_10.4.3.4"><label>10.4.3.4</label><title>Mass of divided sample</title></section><section id="sec_10.4.3.5"><label>10.4.3.5</label><title>Procedure</title></section></section><section id="sec_10.4.4"><label>10.4.4</label><title>Manual riffle-division method</title><section id="sec_10.4.4.1"><label>10.4.4.1</label><title>General</title></section><section id="sec_10.4.4.2"><label>10.4.4.2</label><title>Selection of riffle divider</title></section><section id="sec_10.4.4.3"><label>10.4.4.3</label><title>Mass of divided sample</title></section><section id="sec_10.4.4.4"><label>10.4.4.4</label><title>Procedure</title></section></section></section><section id="sec_10.5"><label>10.5</label><title>Preparation of test samples for chemical analysis</title><section id="sec_10.5.1"><label>10.5.1</label><title>Mass and particle size</title></section><section id="sec_10.5.2"><label>10.5.2</label><title>Preparation to 250 µm nominal top size</title></section><section id="sec_10.5.3"><label>10.5.3</label><title>Final preparation</title><section id="sec_10.5.3.1"><label>10.5.3.1</label><title>Case 1</title></section><section id="sec_10.5.3.2"><label>10.5.3.2</label><title>Case 2</title></section><section id="sec_10.5.3.3"><label>10.5.3.3</label><title>Case 3</title></section></section><section id="sec_10.5.4"><label>10.5.4</label><title>Grinding to 100 µm or 160 µm nominal top size</title><section id="sec_10.5.4.1"><label>10.5.4.1</label><title>General</title></section><section id="sec_10.5.4.2"><label>10.5.4.2</label><title>Type of grinder</title></section><section id="sec_10.5.4.3"><label>10.5.4.3</label><title>Selection of material of construction for grinder</title></section><section id="sec_10.5.4.4"><label>10.5.4.4</label><title>Dry grinding</title></section><section id="sec_10.5.4.5"><label>10.5.4.5</label><title>Wet grinding</title></section></section><section id="sec_10.5.5"><label>10.5.5</label><title>Distribution of samples for chemical analysis</title></section></section><section id="sec_10.6"><label>10.6</label><title>Preparation of test samples for moisture determination</title></section><section id="sec_10.7"><label>10.7</label><title>Preparation of test samples for size determination</title></section><section id="sec_10.8"><label>10.8</label><title>Preparation of test samples for physical testing</title><section id="sec_10.8.1"><label>10.8.1</label><title>Selection of sample preparation procedure</title><section id="sec_10.8.1.1"><label>10.8.1.1</label><title>General</title></section><section id="sec_10.8.1.2"><label>10.8.1.2</label><title>Split use of sample</title></section><section id="sec_10.8.1.3"><label>10.8.1.3</label><title>Combination of split use and multiple use of sample</title></section></section><section id="sec_10.8.2"><label>10.8.2</label><title>Extraction of test samples</title><section id="sec_10.8.2.1"><label>10.8.2.1</label><title>General</title></section><section id="sec_10.8.2.2"><label>10.8.2.2</label><title>Test sample for tumble test</title><section id="sec_10.8.2.2.1"><label>10.8.2.2.1</label><title>General </title></section><section id="sec_10.8.2.2.2"><label>10.8.2.2.2</label><title>Pellets</title></section><section id="sec_10.8.2.2.3"><label>10.8.2.2.3</label><title>Sinter and lump ores</title></section></section><section id="sec_10.8.2.3"><label>10.8.2.3</label><title>Test sample for bulk density test</title></section><section id="sec_10.8.2.4"><label>10.8.2.4</label><title>Test samples for physical tests other than tumble test and bulk density test</title><section id="sec_10.8.2.4.1"><label>10.8.2.4.1</label><title>General</title></section><section id="sec_10.8.2.4.2"><label>10.8.2.4.2</label><title>Blast-furnace pellets</title></section><section id="sec_10.8.2.4.3"><label>10.8.2.4.3</label><title>Direct-reduction pellets</title></section><section id="sec_10.8.2.4.4"><label>10.8.2.4.4</label><title>Sinter and blast-furnace lump ores</title></section><section id="sec_10.8.2.4.5"><label>10.8.2.4.5</label><title>Direct-reduction lump ores</title></section></section></section><section id="sec_10.8.3"><label>10.8.3</label><title>Reserve samples</title></section></section></section><section id="sec_11"><label>11</label><title>Packing and marking of samples</title></section></section><section id="sec_A"><label>Annex A</label><title>Inspection of mechanical sampling systems (informative)</title><section id="sec_A.1"><label>A.1</label><title>Purpose of inspections</title></section><section id="sec_A.2"><label>A.2</label><title>Mechanical and operational inspections</title></section><section id="sec_A.3"><label>A.3</label><title>Control charts</title><section id="sec_A.3.1"><label>A.3.1</label><title>General</title></section><section id="sec_A.3.2"><label>A.3.2</label><title>Sampling ratio</title></section><section id="sec_A.3.3"><label>A.3.3</label><title>Extraction ratio</title></section></section></section><section id="sec_B"><label>Annex B</label><title>Formulae for number of increments (normative)</title><section id="sec_B.1"><label>B.1</label><title>Symbols</title></section><section id="sec_B.2"><label>B.2</label><title>Derivation</title></section></section><section id="sec_C"><label>Annex C</label><title>Alternative methods of taking the reference sample (informative)</title><section id="sec_C.1"><label>C.1</label><title>Principles of alternative method</title></section><section id="sec_C.2"><label>C.2</label><title>Layout of ore flow diversion</title></section><section id="sec_C.3"><label>C.3</label><title>Schemes for diversion</title><section id="sec_C.3.1"><label>C.3.1</label><title>Scheme 1</title></section><section id="sec_C.3.2"><label>C.3.2</label><title>Scheme 2</title></section><section id="sec_C.3.3"><label>C.3.3</label><title>Scheme 3</title></section><section id="sec_C.3.4"><label>C.3.4</label><title>Scheme 4</title></section></section></section><section id="sec_D"><label>Annex D</label><title>Procedure for determining the minimum mass of divided gross sample for size determination using other mechanical division methods (normative)</title><section id="sec_D.1"><label>D.1</label><title>General</title></section><section id="sec_D.2"><label>D.2</label><title>Procedure</title></section><section id="sec_D.3"><label>D.3</label><title>Examples of calculation of the minimum mass of divided gross sample for size determination</title><section id="sec_D.3.1"><label>D.3.1</label><title>Example 1</title></section><section id="sec_D.3.2"><label>D.3.2</label><title>Example 2</title></section><section id="sec_D.3.3"><label>D.3.3</label><title>Example 3</title></section></section></section><section id="sec_E"><label>Annex E</label><title>Riffle dividers (normative)</title></section><section id="sec_bibl"><title>Bibliography</title></section></toc>