Foreword

Hauptteil

1Scope

2Normative references

3Terms and definitions

4Principle

5Apparatus

5.1Eluent supply

5.2Pump

5.3Injection system

5.4Separation columns

5.5Column temperature control

5.6Detector

6Reagents

7Calibration of the apparatus

7.1General

7.2Specification for the calibration standards

7.3Preparation of the calibration solutions for injection

7.4Conditions for calibration runs

7.5Measurement of elution volume

7.6Plotting the calibration curve

8Sampling

9Preparation for the test

9.1Preparation of the injection solution

9.2Preparation of the apparatus

10Analytical parameters

11Data acquisition and evaluation

11.1General

11.2Calculation of the net chromatogram from the raw data

11.2.1Determination of the baseline

11.2.2Correction of the measured values and of the net chromatogram

11.2.3Evaluation limits

11.3Calculation of the average values

11.4Calculation of the distribution curves

12Precision

12.1General

12.2Repeatability

12.3Reproducibility

13Test report

13.1General

13.2General data on the equipment and settings

13.2.1Data on the equipment used

13.2.2Calibration

13.2.3Evaluation

13.3Special data on the sample