ASTM D 6331:2024

1.1 This test method 2 covers a method for the measurement of particulate matter (dust) concentration in emission gases in concentrations below 20 mg/m³ under standard conditions, with special emphasis of concentrations around 5 mg/m³. 1.2 To meet the requirements of this test method, the particulate sample is weighed to a specified level of accuracy. At low dust concentrations, this is achieved by: 1.2.1 Precise and repeatable weighing procedures, 1.2.2 Using low tare weight weighing dishes, 1.2.3 Extending the sampling time at conventional sampling rates, or 1.2.4 Sampling at higher rates at conventional sampling times (high-volume sampling). 1.3 This test method differs from Test Method D3685/D3685M by requiring the mass measurement of filter blanks, specifying weighing procedures, and requiring monitoring of the flue gas flow variability over the testing period. It requires that the particulate matter collected on the sample filter have a mass at least five times a positive mass difference on the filter blank. High volume sampling techniques or an extension of the sampling time may be employed to satisfy this requirement. This test method has tightened requirements on sampling temperature fluctuations and isokinetic sampling deviation. This test method has eliminated the in-stack filtration technique. 1.4 This test method may be used for calibration of automated monitoring systems (AMS). If the emission gas contains unstable, reactive, or semi-volatile substances, the measurement will depend on the filtration temperature. 1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

13.040.99